Chemistry
Regulations of the student laboratory of analytical chemistry (doc, 31 KB)Examples of computational exercises (in English, with solutions) (doc, 439 KB)Syllabus for 'Analytical chemistry' (Chemistry, 1st year, 2nd semester) (doc, 68 KB)Syllabus for 'Selected special techniques in chemical analysis' (Chemistry, optional, 1st year, 2nd semester) (doc, 60 KB)Syllabus for the full-semester program (Erasmus) (doc, 28 KB)Syllabus for the half-semester program (Erasmus) (doc, 27 KB)Analytical Chemistry course - Laboratory schedule (doc, 50 KB)'Selected special techniques in chemical analysis' (Chemistry, optional, 1st year, 2nd semester) - the schedule (doc, 39 KB)Safety rules in laboratory (doc, 118 KB)
Instructions for laboratory tasks
- Safety in laboratory, preparation of glass, pipetting, heating etc. (file doesn't exist, - KB)
Classical qualitative analyses
- 1A. Solubility product, factors affecting solubility. (pdf, 437KB)
- 1B. Identification reactions – precipitation reactions, complex formation reactions, oxidation-reduction reactions (pdf, 437KB)
- 2. Spot test analysis (pdf, 270KB)
- 3. Microcrystalline analysis (pdf, 260KB)
- 4. Alloys analysis (pdf, 337KB)
- 5. Analysis of non-metallic ions-anions (pdf, 410KB)
- 6. Analysis of the simple solid sample (pdf, 223KB)
- 7. Amphoteric properties of hydroxides (pdf, 357KB)
Classical quantitative analyses
- Preparation and titration of NaOH solution. This titrant will be used in exercises nos. 8, 9 and 15 (pdf, 445KB)
- 8a. Acid-base titration. A/ Vitamin C (askorbinic acid) in tablets (pdf, 283KB)
- 8b. Acid-base titration. B/ Ibuprofen in tablets (pdf, 284KB)
- 8c. Acid-base titration. C/ Aspirin (acetylsalicylic acid) in tablets (pdf, 295KB)
- 9. Determination of NaCl using ionic exchangers (pdf, 303KB)
- 10. Gravimetric determination of nickel in alloys (pdf, 351KB)
- 10A. Gravimetric determination of copper as CuSCN (pdf, 417KB)
- 11. Argentometric determination of chlorides in food by the method of Mohr. Comparison of the Fajans, Mohr, and Volhard recipes (pdf, 340KB)
- 12. Redox. Iodometric determination of glucose (pdf, 243KB)
- 12A. Redox. Manganometric determination of iron (pdf, 428KB)
- 13. Redox. Iodometric determination of copper in alloys (pdf, 264KB)
- 14. Complexometric determination of calcium and magnesium in the same sample (pdf, 325KB)
- 14A. Complexometric determination of nickel (pdf, 304KB)
- 14B. Complexometric determination of bismuth (pdf, 378KB)
Instrumental (physicochemical) analyses
- 15. Determination of H3PO4 or citric acid by volumetric and pH-metric methods (pdf, 306KB)
- 16. Quantitative volumetric analysis with conductometric detection of the end-point (pdf, 551KB)
- 17. Electrogravimetric determination of copper and lead in alloys (pdf, 534KB)
- 18. Determination of total fat content in natural products and foodstuffs – the extraction method (pdf, 493KB)
- 19. Determination of the alcohol content in beverages - distillation method (pdf, 556KB)
- 20. Thin-layer chromatography of acid-base indicators (pdf, 457KB)
- 21. Colorimetric determination of Fe(III) using the thiocyanate method (pdf, 571KB)
- 22. Ashing of organic samples and determination of Zn and Fe using ICP-AES method (pdf, 471KB)
- 23. Turbidimetry – Determination of sulphates and chlorides in natural surface waters (pdf, 539KB)
- 24. UV-Vis spectra of plant dyes. Colors (pdf, 352KB)
- 28. Determination of nitrogen in fertilizers by the Kjeldahl method. (pdf, 306KB)
- 29. Determination of carbonate in minerals by gravimetric method. (pdf, 340KB)
Various useful files
- Glass and equipments used in the laboratory - photos and names (both in Polish and English) (pdf, 1 359KB)
- Table - Dissociation constants of acids (xls, 51KB)
- Table - Solubility constants (xls, 52KB)
- Table - Stability constants of complexes (xls, 55KB)
- Table - Standard potentials of redox half-reactions (xls, 58KB)
- Titration curve of mono-, di- and triproton acids (xls, 76KB)
- A list of instrumental methods of chemical analysis - their advantages and disadvantages (in English) (doc, 51KB)
- International Alcoholometric Tables (pdf, 4 960KB)